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Hochtemperatur-In-situ-Elektronenrückstreubeugung von WC-Co-Hartmetallen für Temperaturen bis zu 1000°C

€25.00

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Product Details
Description

Kobalt kommt in zwei Kristallstrukturen vor: hexagonal dichtest gepackt (hdp) und kubisch flächenzentriert (kfz), die in Werkstoffen wie WC-Co-Hartmetallen bei Raumtemperatur koexistieren. Je nach vorhandener Kristallstruktur ändern sich die mechanischen Eigenschaften und die Bildung von Mik-rodefekten wird beeinflusst. In der vorliegenden Arbeit wird die hdp/kfz-Co-Phasenumwandlung von WC-Co-Hartmetallen mittels Hochtemperatur- Elektronenrückstreubeugungsmessungen untersucht. Die Pha-senanalyse an der Probenoberfläche wurde in-situ während einer schrittweisen Erwärmung von Raum-temperatur bis 1000 °C durchgeführt. Die untersuchten Hartmetallsorten unterscheiden sich in der WC-Korngröße von 0,7 μm und 2,0 μm und dem Co-Gehalt von 10 Gew.-% und 12 Gew.-%. Die Elektronen-rückstreubeugungsmessung an WC-10 Gew.-% Co-Hartmetallen mit Co-Stegbreiten größer als 300 nm ermöglichten eine eindeutige Identifizierung der Co-Phasen. Messungen oberhalb von 800 °C waren auf-grund der Diffusion und der Abscheidung des Co-Binders aus dem WC-Skelett auf die WC-Körner nicht zielführend. Aussagekräftige Ergebnisse wurden für WC-Co-Hartmetalle bis 700 °C erzielt.

Reference: WP-2023-247

Title: Hochtemperatur-In-situ-Elektronenrückstreubeugung von WC-Co-Hartmetallen für Temperaturen bis zu 1000°C
Author(s): K. Maier, B. Sartory, T. Klünsner, C. Czettl, D. Brandl
DOI: 10.48447/WP-2023-247
Event: Werkstoffprüfung 2023: Werkstoffe und Bauteile auf dem Prüfstand - Tagung
Year of publication: 2023
Publication type: conference paper (PDF)
Language: German
Keywords: Hochtemperatur-EBSD,WC-Co-Hartmetall,Co-Phasenumwandlung

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Einfluss der PEO-Oberfläche auf das Ermüdungs- und Korrosionsermüdungsverhalten der Mg-Zn-Ca-Legierung ZX10 ...

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Analyse der Schädigungsentwicklung des in kerntechnischen Anlagen verwendeten Stahls X6CrNiNb18-10 bei einsatztypischen Temperaturen

Publication type: conference paper (PDF)

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